FIELD: production of polymethyl siloxane liquids which are used as heat carrier, working liquids for hydrosystem and as antifrothing agents for petroleum oil. SUBSTANCE: polymethyl siloxane liquids are prepared by hydrolysis of mixture which comprises dimethyldichlorosilane and trimethylchlorosilane. The process is followed by neutralization of product of hydrolysis by 4-30 % suspension of chalk in polymethyl siloxane liquid, mass ratio of product of hydrolysis and chalk being 1:0.0015-0.002, respectively. Product is then separated, affected by catalytic rearrangement and then distilled into fractions. EFFECT: improved efficiency of the method. 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING POLYMETHYLSILOXANE LIQUIDS | 1996 |
|
RU2111980C1 |
PROCESS FOR PREPARING POLYETHYLSILOXANE FLUIDS | 1992 |
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METHOD OF SYNTHESIS OF MONOMERS CONTAINING FUNCTIONAL GROUPS FOR POLYETHYLSILOXANE LIQUIDS SYNTHESIS | 1992 |
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PROCESS FOR PREPARING OLIGOORGANOSILOXANES | 0 |
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METHOD FOR OBTAINING OLIGOMETHYLSILOXANES OF BRANCHED STRUCTURE | 0 |
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METHOD OF PREPARING OF POLYETHYLSILOXANE LIQUIDS | 1992 |
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METHOD OF HYDROLYSIS OF DIMETHYL DICHLOROSILANE | 1999 |
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METHOD FOR PRODUCTION OF POLYORGANOSILOXANE VARNISH | 1995 |
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METHOD OF PRODUCING OLIGODIMETHYLSILOXANES | 2013 |
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RU2513022C1 |
METHOD FOR PREPARING BRANCHED POLYMETHYLSILOXANES | 0 |
|
SU1641833A1 |
Authors
Dates
1998-03-20—Published
1996-03-28—Filed