FIELD: heat carriers and working liquids for hydraulic systems. SUBSTANCE: polymethylsiloxane liquids are prepared by hydrolysis of mixture of methyl trichlorosilane, dimethyl dichlorosilane and trimethyl chlorosilane followed by neutralization of hydrolysis product with soap as 5-30% suspension in polymethylsiloxane liquid at hydrolysis product to chalk weight ratio of 1: 0.0015-0.0020, filtration of hydrolysis product, catalytic regrouping of the resulting filtrate and fractionation. The claimed method makes it possible to reduce amounts of chalk and losses of hydrolysis product, and improve working conditions. EFFECT: more efficient preparation method. 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PRODUCTION OF POLYMETHYL SILOXANE LIQUIDS | 1996 |
|
RU2107075C1 |
PROCESS FOR PREPARING POLYETHYLSILOXANE FLUIDS | 1992 |
|
RU2048486C1 |
METHOD OF SYNTHESIS OF MONOMERS CONTAINING FUNCTIONAL GROUPS FOR POLYETHYLSILOXANE LIQUIDS SYNTHESIS | 1992 |
|
RU2027718C1 |
METHOD FOR PRODUCTION OF POLYORGANOSILOXANE VARNISH | 1995 |
|
RU2108347C1 |
METHOD OF PREPARING OF POLYETHYLSILOXANE LIQUIDS | 1992 |
|
RU2034865C1 |
METHOD OF HYDROLYSIS OF DIMETHYL DICHLOROSILANE | 1999 |
|
RU2175333C2 |
METHOD FOR OBTAINING OLIGOMETHYLSILOXANES OF BRANCHED STRUCTURE | 0 |
|
SU1689381A1 |
METHOD OF PREPARING OLIGOMETHYL-GAMMA-TRIFLUOROPROPYLSILOXANES | 2004 |
|
RU2268902C1 |
METHOD OF SYNTHESIS OF MONOMERS CONTAINING FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLSILOXANE LIQUIDS | 1992 |
|
RU2036926C1 |
PROCESS FOR PREPARING OLIGOORGANOSILOXANES | 0 |
|
SU1081179A1 |
Authors
Dates
1998-05-27—Published
1996-03-28—Filed