FIELD: chemistry of polymers, more particularly, production of polysulfide oligomers. SUBSTANCE: 2,2'- dichlorodiethylformal is prepared by reacting 1- chloromethyl-2'-chloroethyl ether with ethylene oxide in the presence of catalytic amount of zinc chloride at temperatures from -10 C to +10 C, to obtain product with high yield under mild conditions. EFFECT: simplified preparation method. 2 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING 2,2'-DICHLORODIETHYLFORMAL | 2013 |
|
RU2522332C1 |
METHOD OF PRODUCING 2,2'-DICHLORODIETHYLFORMAL | 2010 |
|
RU2439049C1 |
DI-(β-CHLOROETHYL)FORMAL SYNTHESIS METHOD | 2008 |
|
RU2398756C2 |
METHOD FOR PRODUCTION OF POLYSULFIDE OLIGOMERS | 1995 |
|
RU2099361C1 |
METHOD OF SULFURIC ACID WASTES UTILISATION | 2012 |
|
RU2500614C1 |
METHOD OF THE VACUUM RECTIFICATION OF ETHYLENE CHLOROHYDRIN | 2004 |
|
RU2277082C1 |
PROCESS FOR PREPARING BETA-CHLORETHYL ESTER OF CHLOROSULFONIC ACID | 0 |
|
SU1087517A1 |
SYNTHETIC LATEX AND METHOD FOR PRODUCTION THEREOF | 2012 |
|
RU2496803C1 |
0 |
|
SU302343A1 | |
METHOD OF PRODUCING 2-CHLORALKYLDICHLOROPHOSPHITES | 0 |
|
SU1397452A1 |
Authors
Dates
1999-12-27—Published
1998-07-07—Filed