FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing 2,2'-dichlorodiethylformal. The method is realised by reacting ethylene chlorohydrin and paraformaldehyde in the presence of magnesium sulphate or magnesium chloride crystalline salt. 2,2'-dichlorodiethylformal is extracted by salting out the organic phase by saturating with magnesium salt solution. Excess ethylene chlorohydrin is then distilled from the organic phase.
EFFECT: low concentration of ethylene chlorohydrin in synthesis wastes, low expenses on recycling wastes, high environmental safety of production.
4 cl, 2 ex
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Authors
Dates
2012-01-10—Published
2010-04-12—Filed