FIELD: chemical industry. SUBSTANCE: described is new method of preparing new compound such as diphenyl di[(1-ethyl-1-alumocyclopent-3- yl)methyl] silane by reacting diphenyldiallyl silane with triethyl aluminium in the presence of zirconadene dichloride catalyst in argon atmosphere in aliphatic solvent under normal conditions for 6-10 hours. EFFECT: more efficient preparation method. 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING 1-ETHYL-3- (TRIALKYLSILYL)ALUMACYCLOPENTANES | 1999 |
|
RU2157812C1 |
METHOD OF PREPARING 1-(DIALKYLAMINO)-2- (TRIALKYLSILYL)ALUMACYCLOPROPANES | 1999 |
|
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METHOD OF PREPARING 1-ETHYL-2-(TRIALKYLSILYL) ALUMACYCLOPROPANES | 1999 |
|
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METHOD OF PREPARING 1-ALKOXY-2- (TRIALKYLSILYL)ALUMACYCLOPROPANES | 2000 |
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METHOD OF PREPARING 1-VINYL-1-METHYL-3-ALKYLSILACYCLOPENTANES | 2000 |
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METHOD FOR PREPARING 1-ETHYL-3,3-DIALKYL-6,7-FULLERENO[60]CYCLOHEPTA-2-OX-1-ALANES | 2002 |
|
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METHOD OF SYNTHESIS OF SUBSTITUTED 1-ETHYLALUMO-CYCLOPENTANES | 2001 |
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METHOD FOR PREPARING 1-ETHYL-3-METHYL-3-PHENYL-(ETHYL-, CYCLOPROPYL-)-4-ALKYLIDENECYCLOHEPTA-2-OXALANES | 2002 |
|
RU2213745C1 |
METHOD OF COMBINED PREPARATION OF 1-ETHYL-2-ARYL, 1- ETHYL-3-ARYL, 1-ETHYL-2,4-DIARYL, 1-ETHYL-2,5-DIARYL ALUMACYCLOPENTANES AND 1-ETHYL-2-ARYL ALUMACYCLOPROPANES | 1999 |
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METHOD OF SYNTHESIS OF ALK-4Z-EN-1-OLS | 2001 |
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RU2200147C1 |
Authors
Dates
2000-07-27—Published
1999-03-24—Filed