DINITRILES HYDROGENATION PROCESS Russian patent published in 2002 - IPC

Abstract RU 2181716 C2

FIELD: industrial organic synthesis. SUBSTANCE: hydrogenation of aliphatic dinitriles into corresponding aminonitriles is effected continuously in presence of hydrogenation catalyst not soluble in reaction mixture. Gas contained in the reaction mixture is separated at the reactor outlet, in the zone wherein gas-liquid transfer is limited or entirely absent. Reaction mixture with reduced gas phase level is fed into hydrogenation reactor. Part of reaction mixture is withdrawn from above-indicated reaction zone after solid phase separation in liquid/solid separation zone. Solid phase obtained by settling in hydrogenation reactor (reactor residence time less than 30 min) is recycled into liquid/solid separation zone. EFFECT: avoided deactivation of catalyst. 16 cl, 2 dwg, 1 tbl, 3 ex

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RU 2 181 716 C2

Authors

Bosha Vensan

Lekont Filipp

Roshett Daniel'

Sever Lionel'

Dates

2002-04-27Published

1998-11-19Filed