FIELD: non-ferrous metallurgy, in particular, metallurgy of noble metals. SUBSTANCE: method involves treating chloric solutions of noble metals with sodium nitrite in the process of obtaining rhodium ammonium-sodium salts, with more than 50% of sodium nitrite being reproduced; treating resultant gaseous mixture containing nitric oxide with sodium hydroxide in two-four sequentially connected absorbers. Prior to treatment with sodium hydroxide, gaseous mixture is treated with oxidizer such as air, oxygen, nitric acid, hydrogen peroxide. EFFECT: increased efficiency and simplified process. 2 cl, 3 ex
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