METHOD FOR PREPARING DIBENZTHIAZOLYL DISULFIDE Russian patent published in 2003 - IPC

Abstract RU 2206567 C1

FIELD: organic chemistry, chemical technology. SUBSTANCE: invention relates to method for preparing dibenzthiazolyl disulfide by oxidation of alkaline solution of 2- mercaptobenzthiazole with oxygen in the presence of cobalt phthalocyanine as a catalyst at 50 C. Process is carried out in 3-10-fold excess of 2-mercaptobenzthiazole by solubility in weakly alkaline medium where concentration of alkaline metal hydroxide is 0.35-1.0 weight % in the presence of cobalt disulfophthalocyanine as a catalyst taken in amount (3-5) x 10-4 mole per 1 mole of 2-mercaptobenzthiazole. EFFECT: simplified method for preparing. 4 ex

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RU 2 206 567 C1

Authors

Kalija O.L.

Mekhrjakova N.G.

Kravchuk O.V.

Dates

2003-06-20Published

2001-11-26Filed