FIELD: organic chemistry, chemical technology. SUBSTANCE: invention relates to method of synthesis of 5-chloro-2,1,3-benzothiadiazole by interaction of 4-chloro-1,2-phenylenediamine with thionyl chloride in the presence of catalytic amount of dimethylformamide in organic solvent medium at 125-130 C. Invention provides increase of yield of 5-chloro-2,1,3-benzothiadiazole. EFFECT: simplified method, increased yield. 4 ex
Authors
Dates
2003-04-27—Published
2001-07-04—Filed