FIELD: medicine, sanitary toxicology. SUBSTANCE: patient's urinary sample should be supplemented with sodium chloride salting out agent to perform its alkalization with 10%-sodium hydroxide solution up to pH = 8 - 10, carry out extraction of chlorobenzene out of the sample due to its extraction with heptane, separate the extract due to centrifuging, carry out its studying by gas chromatography assay. As for chlorobenzene quantity it should be established by calibrating diagram. Optimal centrifuging modes are those of 2700 rot. /min at 15 min centrifuging terms. EFFECT: higher sensitivity and accuracy of detection. 1 cl, 1 ex, 3 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF BLOOD DICHLOROBROMOMETHANE MEASUREMENT | 2009 |
|
RU2416798C1 |
METHOD FOR QUANTITATIVE DETERMINATION OF URINARY 2-CHLOROPHENOL | 2001 |
|
RU2190854C1 |
METHOD OF QUANTITATIVE DETERMINATION OF HEXACHLOROBENZENE IN BLOOD BY METHOD OF GAS CHROMATOGRAPHIC ANALYSIS | 2016 |
|
RU2613306C1 |
METHOD OF QUANTITATIVE DETERMINATION OF CHLOROFORM AND TETRA- CHLOROMETHANE IN BLOOD | 2000 |
|
RU2163379C1 |
METHOD FOR QUANTITATIVE DETERMINATION OF CHLOROFORM AND 1,2- DICHLOROETHANE IN URINE | 1999 |
|
RU2151395C1 |
METHOD FOR QUANTITATIVE DETERMINATION OF N-NITROSODIMETHYLAMINE AND N-NITROSODIETHYLAMINE IN URINE BY GAS CHROMATOGRAPHIC ANALYSIS | 2013 |
|
RU2521711C1 |
METHOD FOR QUANTITATIVE DETERMINATION OF FURAN AND METHYLFURAN IN BLOOD BY GAS CHROMATOGRAPHIC ANALYSIS WITH MASS SELECTIVE DETECTION | 2023 |
|
RU2813866C1 |
METHOD OF DETERMINING AROMATIC HYDROXY DERIVATIVE ESTERS | 1997 |
|
RU2142125C1 |
METHOD OF URINE PHENOL QUANTITATIVE DETERMINATION | 2001 |
|
RU2200958C1 |
METHOD OF DETERMINING 2,6-BIS[BIS(BETA-HYDROXYETHYL)AMINO]-4,8-DI-N-PYPERIDINO-PYRIMIDO(5,4-D)PYRIMIDINE IN BIOLOGICAL MATERIAL | 2006 |
|
RU2322674C1 |
Authors
Dates
2004-04-10—Published
2002-08-20—Filed