METHOD FOR PREPARING ADJOENE (Z)- AND (E)-ISOMERS IN RATIO 2:1 Russian patent published in 2004 - IPC

Abstract RU 2239630 C1

FIELD: chemical technology.

SUBSTANCE: invention relates to a method for preparing mixture of (Z)- and (E)-isomers of adjoin in the ratio 2:1. Solution of synthetic illicit in n-butanol is kept for 6 days at temperature 21-23oC followed by, if necessary, separation of isomers by method of preparative HPLC.

EFFECT: improved preparing method.

1 tbl, 1 dwg, 1 ex

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RU 2 239 630 C1

Authors

Zalepugin D.Ju.

Kozlova A.E.

Korolev V.L.

L'Vov I.A.

Mishin V.S.

Poljakov V.S.

Til'Kunova N.A.

Tolokonnikova Ju.V.

Chernyshova I.V.

Dates

2004-11-10Published

2003-05-12Filed