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2 285 005

(13)

(51)

IPC

C07D471/18(2006-01-01)

(21) (22)

Application

2005119201/04, 2005-06-22

(24)

Start date

2005-06-22

(22)

Actual filing date

2005-06-22

(45)

Published

2006-10-10

(72)

Inventor

Kuznetsov Anatolij IvanovichAzzheurova Irina Anatol'Evna

(73)

Holder

Moskovskaja Gosudarstvennaja Akademija Tonkoj Khimicheskoj Tekhnologii Im. M.V. Lomonosova

METHOD FOR PREPARING 3,6-DIAZAHOMOADAMANTANE Russian patent published in 2006 - IPC C07D471/18

Abstract RU 2285005 C1

FIELD: organic chemistry, chemical technology, virology.

SUBSTANCE: invention relates to a new method for synthesis of a novel compound - 3,6-diazahomoadamantane of the formula: . Compounds of 3,6-diazahomoadamantane class possess an antiviral effect comparable with antiviral effect of aminoadamantane, elicit strychnine-like activity and show bactericidal, fungicide and algicidal properties and can be used as an antiviral preparation. Method for synthesis of 3,6-diazahomoadamantane involves interaction of 1-phenylthio-3,6-diazahomoadamantane-9-one with 65-66% hydrazine hydrate at boiling to form 1-phenylthio-3,6-diazahomoadamantane-9-one hydrazone that is subjected for reduction in Kizhner-Wolf reaction by alloying with alkali and then 1-phenylthio-3,6-diazahomoadamantane is desulfurized with Raney nickel in isopropyl alcohol at boiling.

EFFECT: improved method of synthesis.

2 cl, 1 ex

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RU 2 285 005 C1

Authors

Kuznetsov Anatolij Ivanovich

Azzheurova Irina Anatol'Evna

Dates

2006-10-10—Published

2005-06-22—Filed