FIELD: chemical technology.
SUBSTANCE: invention relates to a method for preparing a binding agent for a dry film photoresist of aqueous-alkaline development used in preparing a picture in making printed boards in radio- and electronic industry and as a component of paint and varnish covers and glues. Invention describes a single-step method for preparing a binding agent for a dry film photoresist of aqueous-alkaline development. At the first step method involves the copolymerization reaction of styrene with maleic anhydride in acetone medium in the presence of azo-bis-isobutyric acid dinitrile and hydroquinone at temperature 54-72°C for 2.5-3.0 h. At the second step method involves addition of 28.0-32.0 mas. p. p. of n-butanol to the reaction mixture and distilling off of 15.0-20.0 mas. p. p. of acetone followed by carrying out esterification of the copolymerization product at temperature 64-74° for 90-120 h. Prepared dry film photoresists of aqueous-alkaline development possess high stability (9-10 h) and enhanced galvanic-chemical resistance.
EFFECT: improved preparing method, improved and valuable properties of binding agent.
1 tbl, 6 ex
Title | Year | Author | Number |
---|---|---|---|
PHOTOPOLYMERIZABLE COMPOSITION FOR PHOTORESIST FILM | 1999 |
|
RU2163724C1 |
DRY FILM PHOTORESIST | 2000 |
|
RU2190869C2 |
DRY FILM PHOTORESIST | 2000 |
|
RU2190870C2 |
DRY FILM PHOTORESIST | 2000 |
|
RU2190871C2 |
0 |
|
SU1669922A1 | |
0 |
|
SU408555A1 | |
DRY-FILM PHOTORESIST OF WATER-ALKALINE DEVELOPMENT | 1986 |
|
SU1342280A1 |
PHOTOPOLYMERIZING COMPOSITION FOR DRY FILM PHOTORESIST | 1985 |
|
SU1295930A1 |
METHOD OF PRODUCING CARBOXYL CATIONITES | 0 |
|
SU1392076A1 |
METHOD OF OBTAINING COPOLYMER OF STYRENE AND N-(N-OXYPHENYL) MALEIMIDE | 0 |
|
SU1162820A1 |
Authors
Dates
2006-11-10—Published
2005-03-28—Filed