FIELD: production of mono-crystals of dielectrics and semiconductors by oriented crystallization at drawing ingot upwards from melts, possibly manufacture of semiconductor and opto-electric mono-crystalline materials.
SUBSTANCE: method comprises steps of drawing mono-crystal from inner crucible having opening or openings and arranged inside outer crucible; setting initial compositions of melts in inner and outer crucibles; as crystal is drawn, moving inner crucible relative to outer one with use of computer at rate determined according to formula: v =(m-1)(dmc/dt)/(ρL x Sin)+(dmc/dt)/(ρL x So) where v - motion speed of inner crucible relative to outer one, "+" - downwards, "-" - upwards; m = dmf /dmc - replenishing parameter; mc - crystal mass; mf - mass of melt fed from outer crucible into inner crucible; t - time; ρL - melt density; Sin - surface area of cross section of inner crucible; So - surface area of cross section of outer crucible.
EFFECT: possibility for controlling composition of mono-crystal and for creating preset lengthwise concentration profile of components of solid solution.
6 cl, 1 ex, 3 dwg
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Authors
Dates
2007-02-10—Published
2005-02-07—Filed