FIELD: organic chemistry, chemistry of terpene compounds.
SUBSTANCE: invention relates to a method for synthesis of 2,10-epoxypinane (β-pinene epoxide). Method involves epoxidation of β-pinene double bond with diluted hydrogen peroxide in an aqueous solution of polar solvents (methanol, N,N-dimethylformamide or acetonitrile) under condition of catalytic effect of manganese sulfate in the presence of sodium hydrocarbonate and salicylic acid. Then epoxide and β-pinene are extracted with aliphatic solvent from the reaction mixture. Polar and aliphatic solvents can be used repeatedly. At final step 2,10-epoxypinane is isolated from crude epoxide by distillation under vacuum with purity degree 95% and the yield 60-70%. Invention provides the development of technological method for synthesis of intermediate compound used in preparing some medicinal, technical and perfume preparations.
EFFECT: improved method of synthesis.
7 ex
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