FIELD: organic chemistry.
SUBSTANCE: claimed method includes catalytic dehydration of commercial 4,5,6,7-tetrahydroindole with 0.1-5.0 % nickel sulfide, carried on alumina, at 250-400°C in solvent in presence or absence of inert gas. Yield of target product is 92-96 % and selectivity is 100 %.
EFFECT: method of high yield and selectivity.
3 cl, 9 ex
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SU777026A1 |
SULPHIDES BASED ALKANES DEHYDROGENATION CATALYSTS | 2017 |
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RU2734917C2 |
Authors
Dates
2007-10-10—Published
2006-05-02—Filed