1-VINYL-2-PHENYLPYRROLE SYNTHESIS METHOD Russian patent published in 2010 - IPC C07D207/323 

Abstract RU 2399615 C1

FIELD: chemistry.

SUBSTANCE: invention relates to an improved method for synthesis of 1-vinyl-2-phenylpyrrole from acetophenoneoxime and acetylene in a dimethyl sulphoxide (DMSO) medium in the presence of potassium hydroxide in amount of 16-25% of the weight of acetophenoneoxime at acetylene pressure equal to atmospheric pressure or close to atmospheric pressure (0.4-0.8 atm), at temperature of 130-150°C for 6-8 hours, with release of the end product through direct vacuum distillation of the residue after predistillation of the DMSO.

EFFECT: high output of end product and increased purity of the product.

9 ex

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RU 2 399 615 C1

Authors

Trofimov Boris Aleksandrovich

Mikhaleva Al'Bina Ivanovna

Petrova Ol'Ga Vital'Evna

Sobenina Ljubov' Nikolaevna

Dates

2010-09-20Published

2009-02-24Filed