FIELD: chemistry, pharmaceutics.
SUBSTANCE: invention relates to method of obtaining catalyst of dehydrating 4,5,6,7-tetrahydroindole into indole. Described is catalyst of dehydrating 4,5,6,7-tetrahydroindole into indole containing nickel sulphide applied on aluminium oxide, catalyst being dopated with sodium and chlorine ions and contains 0.30-2.00% of nickel, 0.20-1.50% of sulphur, 0.10-0.20% of sodium, 0.20-1.00% of chlorine. Also described is method of obtaining catalyst which lies in impregnation of aluminium oxide with nickel salt with further processing with metal sulphide at room temperature in water medium in presence of hydrochloric acid and surface-active substance. Catalyst is isolated by filtration without further washing, dopating of catalyst takes place, and dopants are fixed by means of thermal processing.
EFFECT: increase of mechanical strength and activity of catalyst, as well as increase of its service life.
4 cl, 1 dwg, 10 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR INDOLE PRODUCTION | 2006 |
|
RU2307830C1 |
METHOD FOR PREPARING 4,5,6,7-TETRAHYDROINDOLE | 2005 |
|
RU2297410C2 |
SULPHIDES BASED ALKANES DEHYDROGENATION CATALYSTS | 2017 |
|
RU2734917C2 |
METHOD OF SYNTHESIS OF MERCAPTANES COMPRISING STERIC HINDRANCE PHENOL FRAGMENTS | 2000 |
|
RU2184727C2 |
METHOD OF OBTAINING THIENO(3,2-C) PYRIDINE | 0 |
|
SU1156598A3 |
METHOD OF PURIFYING STYRENE FROM PHENYLACETYLENE IMPURITIES | 2008 |
|
RU2385857C1 |
CATALYST, METHOD OF ITS PREPARATION (VERSIONS) AND PROCESS OF HYDRODESULPHURISATION OF DIESEL FRACTIONS | 2007 |
|
RU2342994C1 |
CATALYST FOR PROCESSING HEAVY OILS AND ITS PREPARATION METHOD | 2015 |
|
RU2593376C1 |
PROCESS FOR PREPARING 2-ALKYL-5,6,7,8-TETRAHYDRO-9,10- ANTHAQUINONE | 1992 |
|
RU2080316C1 |
LEAD SULPHIDE AS ALKANE DEHYDROGENATION CATALYST | 2017 |
|
RU2738935C2 |
Authors
Dates
2009-01-27—Published
2007-05-28—Filed