MANGANESE(II) SUCCINATE TETRAHYDRATE PREPARATION METHOD Russian patent published in 2008 - IPC C07C51/41 C07C55/10 

Abstract RU 2315032 C1

FIELD: organic synthesis.

SUBSTANCE: invention concerns an improved method for synthesis of manganese(II) succinate tetrahydrate wherein manganese(II) carbonate is portionwise added to succinic acid aqueous solution at molar ratio 1:1:4.5, respectively, under continuous stirring and, while maintaining constant temperature 60-65°C, each subsequent portion being added after complete dissolution of preceding manganese carbonate portion, after which desired product is isolated via recrystallization. Method can be used under industrial-scale conditions.

EFFECT: improved purity of product and minimum reactants used.

3 dwg, 2 tbl, 5 ex

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RU 2 315 032 C1

Authors

Karmoliev Rafik Khatimovich

Ruchij Oleg Sergeevich

Dates

2008-01-20Published

2006-04-27Filed