FIELD: chemistry, pharmacology.
SUBSTANCE: climed invention relates to method of obtaining 5-(4-(1,3,5-dithiazinan-5-sulfanyl)-phenyl)-1,3,5-dithiazinan, which finds application as radio protective, anti-tumor, diuretic means, and selective sorbent, and extragent of noble and precious metals. Essence of method lies in interaction of saturated with hydrogen sulfate water solution of formalin with water solution of n-anylin sulfamide (streptocide) with HCI with molar ratio streptocide: formaldehyde: hydrogen sulfate: HCl=1:6:4:4, at temperature 40°C, constant mixing during 2 hours and with further neutralisation with NaOH solution. Output of target product 5-[4-(1,3,5-dithiazinan-5-sulfanyl)-phenyl]-1,3,5- dithiazinan is 93%.
EFFECT: obtaining 5-(4-(1,3,5-dithiazinan-5-sulfanyl)-phenyl)-1,3,5-dithiazinan with high output.
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| Title |
Year |
Author |
Number |
| METHOD FOR SELECTIVE PRODUCTION OF 2-, 3- AND 4-(1,3,5-DITHIAZINAN-5-YL)THIOPHENOLS |
2009 |
- Akhmetova Vnira Rakhimovna
- Rakhimova Elena Borisovna
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2425039C2 |
| "METHOD FOR PREPARATION OF 3-THIA-1,5-DIAZABICYCLO[4,3,1]DECANE AND 5-[4-(1,3,5-DITHIAZINANE-5-YL)BUTYL] 1,3,5-DITHIAZINANE MIXTURE" |
2006 |
- Akhmetova Vnira Rakhimovna
- Vagapov Ruslan Adgamovich
- Nadyrgulova Guzel' Razhapovna
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2323933C1 |
| METHOD FOR SELECTIVE PRODUCTION OF N[3-(1,3,5-DITHIAZINAN-5-YL)PROPYL]-N-[4-(1,3,5-DITHIAZINAN-5-YL)BUTYL]AMINE AND N,N-BIS[3-(1,3,5-DITHIAZINAN-5-YL)PROPYL]-1,4-BUTANE DIAMINE |
2009 |
- Akhmetova Vnira Rakhimovna
- Rakhimova Elena Borisovna
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2409574C2 |
| METHOD OF OBTAINING 5-ACETYLSALICILOYL-1,3,5-DITHIAZINAN |
2007 |
- Akhmetova Vnira Rakhimovna
- Khajrullina Regina Radievna
- Tjumkina Tat'Jana Viktorovna
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2342371C2 |
| "METHOD OF OBTAINING N-[1',3',5'-DITHIAZINAN-5'-YL-CARBONYL]-1,3,5-DITHIAZINAN-5-CARBOXAMIDE" |
2007 |
- Akhmetova Vnira Rakhimovna
- Khajrullina Regina Radievna
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2342370C1 |
| METHOD OF COMBINED PRODUCTION OF MONOMER (N,N-BIS{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}AMINE, N,N-BIS{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}-1,2-ETHANEDIAMINE, 5-{2-[5-{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}-4-METHYL-1,3,5-THIADIAZINAN-3-YL]ETHYL}-1,3,5-DITHIAZINANE) AND DIMERIC BIS-1,3,5-DITHIAZINANES(N-({[(BIS{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}AMINO)METHYL]SULPHANYL}METHYL)-2-[1,3,5-DITHIAZINAN-5-YL]-N-{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}-1-ETHANEAMINE, 3,6,10,13-TETRAKIS-{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}-1,8-DITHIA-3,6,10,13-TETRAAZACYCLOTETRADECANE, 3,5,9,11-TETRAKIS-{2-[1,3,5-DITHIAZINAN-5-YL]ETHYL}-4,10-DIMETHYL-1,7-DITHIA-3,5,9,11-TETRAAZACYCLODODECANE) |
2007 |
- Akhmetova Vnira Rakhimovna
- Rakhimova Elena Borisovna
- Vagapov Ruslan Adgamovich
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2356899C1 |
| METHOD OF PRODUCING N-(1,3,5-DITHIAZINAN-5-YL)-ISONICOTINAMIDE AND N-(2,4,6-TRIMETHYL-1,3,5-DITHIAZINAN-5-YL)-ISONICOTINAMIDE |
2010 |
- Dzhemilev Usein Memetovich
- Akhmetova Vnira Rakhimovna
- Khajrullina Regina Radievna
- Kunakova Rajkhana Valiullovna
|
RU2447072C2 |
| METHOD FOR OBTAINING 5-{2-[5-{2-[1,3,5-DITIAZINAN-5-IL]ETHYL}-4-METHYL-1,3,5-TIADIAZINAN-3-IL]ETHYL}-1,3,5,-DITIAZINAN |
2006 |
- Akhmetova Vnira Rakhimovna
- Rakhimova Elena Borisovna
- Vagapov Ruslan Adgamovich
- Kunakova Rajkhana Valliullovna
- Dzhemelev Usejn Memetovich
|
RU2333910C1 |
| METHOD OF PRODUCING N-(1,3,5-DITHIAZINAN-5-YL)-THIOUREA |
2009 |
- Akhmetova Vnira Rakhimovna
- Khajrullina Regina Radievna
- Kunakova Rajkhana Valiullovna
- Dzhemilev Usein Memetovich
|
RU2414460C1 |
| METHOD FOR SELECTIVE PRODUCTION OF α,ω-BIS-(1,3,5-DITHIAZINAN-5-YL)-3-OXOPENTANE AND α,ω-BIS-(1,3,5-DITHIAZINAN-5-YL)-3,6-DIOXOOCTANE |
2010 |
- Dzhemilev Usein Memetovich
- Rakhimova Elena Borisovna
- Vasil'Eva Inna Vladimirovna
- Akhmetova Vnira Rakhimovna
- Ibragimov Askhat Gabdrakhmanovich
|
RU2459823C2 |
