FIELD: explosive works.
SUBSTANCE: octogene or hexogene are dissolved in organic solvent - cyclohexanone or dimethyl sulfoxide, or acetone, or caprolactam. Spray the solution in the form of an aerosol in a coolant with formation of a powder of the frozen solution. The obtained powder is placed in preliminary cooled sublimator and sublimated from a powder solvent with condensation of its steams at residual pressure 1.2-6.0 Pa, heating to temperature from -3°C to 100 °C with a speed 0.2-1.0°C in a minute and endurance within 4-8 hours before stabilisation of weight of an octogene or hexogene powder.
EFFECT: obtaining of high-quality nanodisperse powder octogene or hexogene with the sizes of particles of 20-60 nanometers, decrease in sensitivity of a powder to mechanical effects.
5 cl, 2 ex, 2 dwg
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Authors
Dates
2009-01-10—Published
2007-03-14—Filed