FIELD: chemistry.
SUBSTANCE: invention concerns organic compound synthesis, particularly method of obtaining 4-biphenylmetacrylate of the formula . Obtained compound is applied in production of heat and weather resistant polymer materials. Claimed method involves dissolution of 4-phenylphenol in 10 wt % aqueous solution of caustic soda, further dosage of acylating agent in the form of metacrylic acid anhydride agent in reaction mix preliminarily cooled to 0-(+5°)C at such rate so as to keep the mix temperature below +10°C at molar ratio of 4-phenylphenol and metacrylic acid anhydride of 1:(1.1-1.5), reaction mix maturing at room temperature with stirring, organic layer extraction, flushing by alkali solution, and drying.
EFFECT: enhanced output of 4-biphenylmetacrylate, admixture content of non-reacted 4-phenylphenol reduced to 0,003-0,005 wt %.
3 cl, 1 tbl, 10 ex
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Authors
Dates
2009-05-20—Published
2007-10-22—Filed