FIELD: chemistry.
SUBSTANCE: invention refers to the methods of warfare irritants disposal, namely to the liquidation and disposal of 2-chloro-1-phenylethanone-1 (chloracetophenone). The method is implemented by the cyclocondensation of 2-chloro-1-phenylethanone-1 with 1-dicyan-2-(2-chlorophenyl)-ethylene in presence of catalytic amounts of piperidine. After filtering, washing and recrystallisation from ethylic alcohol the resulting product - 2-phenyl-3-chloro-4(2-chlorophenyl)-5-cyan-6-amino-1,4-pyran is obtained.
EFFECT: disposal of 2-chloro-1-phenylethanone-1 by its transforming to 2-phenyl-3-chloro-4(2-chlorophenyl)-5-cyan-6-amino-1,4-pyran used in fine organic synthesis, chemistry of physiologically active substances and pharmaceuticals.
2 cl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
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| METHOD OF OBTAINING DERIVATIVES OF 1-BENZOYL-3-(ARYLPYRIDYL) UREA | 0 |
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SU1158043A3 |
| 0 |
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SU417948A3 | |
| METHOD OF PREPARING N-/1-(4-AMINO-2-QUINAZOLINYL)-3-OR-4-PIPERIDYL/-LACTAMS OR THEIR SALTS WITH ACIDS | 0 |
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| METHOD OF PRODUCING 1-CYCLOHEXYL-4-ARYL-4-PIPERIDINCARBOXYLIC ACIDS DERIVATIVES OR THEIR STEREOCHEMICAL ISOMERIC FORMS (VERSIONS) | 0 |
|
SU1230467A3 |
| DERIVATIVES OF AMINO-7-(CHRR)-3H,5H-PYRROLO-[3,2-D]-PYRIMIDINE-4-ONE, METHODS OF THEIR SYNTHESIS AND A METHOD OF SELECTIVE INHIBITION OF MAMMALIAN T-LYMPHOCYTES PROLIFERATION AND NO EFFECTING ON CHRR-LYMPHOCYTES | 1992 |
|
RU2097384C1 |
