METHOD OF UTILISING TOXIC CHLORINE-CONTAINING SUBSTANCE 2-(2-CHLOROBENZYLIDENE)MALONODINITRILE(CS) Russian patent published in 2014 - IPC A62D3/30 A62D101/02 A62D101/22 C07C51/265 C07C63/70 

Abstract RU 2506978 C1

FIELD: chemistry.

SUBSTANCE: invention relates to methods of destruction of toxic substances, namely to utilisation of toxic chlorine-containing substance 2-(2-chlorobenzylidene)malonodinitrile(CS) with obtaining 2-chlorobenzoic acid, which is a marketable product for synthesis of various organic compounds: pesticides, dyes, medications. Method consists in boiling 2-(2-chlorobenylidene)malononitrile in water solution of potassium permanganate for 3-3.5 hours. After that, mixture is kept at room temperature for 14-16 hours, obtained sediment is washed with hot water. Filtrate is evaporated, acidified with 10-15% hydrochloric acid, sediment from filtrate is washed with water and re-crystallised to obtain 2-chlorobenzoic acid.

EFFECT: invention makes it possible to eliminate toxic reagents from technological process and harmful emissions into atmosphere.

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RU 2 506 978 C1

Authors

Sheverdov Vladimir Petrovich

Nasakin Oleg Evgen'Evich

Dates

2014-02-20Published

2012-06-20Filed