FIELD: chemistry.
SUBSTANCE: mixture of monoalkyldiphenylphosphates and dialkylmonophenylphosphates is obtained from reacting phosphorous oxychloride with phenol, after which dichloromonophenylphosphate and monochlorodiphenylphosphate are reacted with aliphatic alcohol in the presence of catalyst - Lewis acid in the absence of a solvent at temperature 60-200°C and pressure from 0.001 to 1.1 bar abs.
EFFECT: design of a new method of producing alkylphenylphosphates and their mixtures, suitable for use plasticisers, lubricants and fireproofing compositions.
16 cl, 17 ex, 5 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR OBTAINING FIRE-RESISTANT HYDRAULIC FLUID BASE | 2020 |
|
RU2751888C1 |
METHOD FOR OBTAINING BASIS OF FLAME-RETARDANT OIL | 2018 |
|
RU2672360C1 |
METHOD FOR CONTINUOUS SYNTHESIS OF ORGANIC CARBONATES OR ORGANIC CARBAMATES AND SOLID CATALYSTS FOR REALISING SAID METHOD | 2009 |
|
RU2447056C1 |
WAYS OF PRODUCTION OF ZILPATEROL AND ITS SALTS | 2008 |
|
RU2442786C2 |
METHOD OF OBTAINING MELAMINE | 2008 |
|
RU2535350C2 |
PROCESS FOR PREPARING DIALKYLARYL PHOSPHATES | 0 |
|
SU1097630A1 |
METHOD FOR OBTAINING MIXED TRIARYL PHOSPHATES | 2018 |
|
RU2670105C1 |
METHOD FOR OBTAINING MONOCHLORACETIC ACID | 2016 |
|
RU2674474C1 |
METHOD OF PRODUCING DIALKYL ETHER OF NAPHTHALENE DICARBOXYLIC ACID (VERSIONS) | 2005 |
|
RU2397158C2 |
METHOD OF PRODUCING ε-CAPROLACTONE AND 1,6-HEXANEDIOL | 2011 |
|
RU2571082C2 |
Authors
Dates
2009-07-20—Published
2004-10-21—Filed