FIELD: metallurgy.
SUBSTANCE: method includes electrolysis from electrolyte made of purified sulphate solutions with insoluble leady anodes. Additionally electrolysis is implemented at electrolyte circulation with keeping of pH 4.5-5.5; temperature is in the range 59.5-65°C and concentration of nickel ions (II) in the initial electrolyte 100-110 g/dm3, and in the waste 40-50 g/dm3. Concentration of nickel ions (II) in the initial electrolyte is kept by means of inlet 20-48% of waste electrolyte from circulation system. Uninterruptedly it is measured pH of solution and it is automatically kept during the electrolysis process by means of acidity adjustment. Electrolyte is fed into interelectrode spacing on surface of bath through graduated branch pipes. In the capacity of cathode there are used reusable cathodes - matrix, implemented from titanium.
EFFECT: method reduction in price, increasing of engineering-and-economical performance of electrolysis process.
4 cl, 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PREPARING ELECTROLYTE FOR ELECTROLYTIC REFINING OF COPPER | 2004 |
|
RU2280106C2 |
METHOD OF ELECTROLYTIC REFINING OF COPPER | 2003 |
|
RU2233913C1 |
METHOD FOR DECOPPERIZATION OF SULFURIC ACID SOLUTIONS OF COPPER ELECTROLYTE PRODUCTION | 2022 |
|
RU2815375C1 |
METHOD OF ELECTROLYTIC REFINING OF NICKEL | 0 |
|
SU1397541A1 |
METHOD OF NICKEL EXTRACTION FROM SPENT CONCENTRATED SOLUTIONS OF ELECTROLESS AND ELECTRIC NICKEL PLATING | 1992 |
|
RU2033480C1 |
METHOD FOR ELECTROLYTIC PREPARATION OF ALKALI | 2008 |
|
RU2366761C1 |
ELECTROEXTRACTION OF COBALT FROM AQUEOUS SOLUTIONS OF COBALT AND MANGANESE SULFATES IN DYNAMIC CONDITIONS | 2017 |
|
RU2677447C2 |
METHOD OF SODIUM HYDROXIDE PREPARATION | 2008 |
|
RU2366762C1 |
METHOD OF STABILIZING SULFATE NICKEL-PLATING ELECTROLYTES | 0 |
|
SU1409680A1 |
ELECTROLYTE COMPOSITION AND METHOD FOR OBTAINING NANOCRYSTALLINE COMPOSITE COATINGS BASED ON NICKEL-PHOSPHORUS-TUNGSTEN SYSTEM | 2021 |
|
RU2792096C1 |
Authors
Dates
2009-07-20—Published
2007-09-28—Filed