METHOD OF REGENERATING SURFACTANTS BASED ON FLUORINATED ACIDS FROM ADSORBENT PARTICLES SATURATED WITH SAID SURFACTANTS Russian patent published in 2010 - IPC C07C51/493 C07C67/54 C07C27/02 C07C53/21 C07C67/08 C07C69/63 

Abstract RU 2382762 C2

FIELD: chemistry.

SUBSTANCE: invention relates to an improved method of regenerating surfactants based on fluorinated acids or their salt from adsorbent particles on which the said surfactants are adsorbed, based on fluorinated acids, involving saturation of adsorbing particles with surfactants based on fluorinated acids or their salt, washing particles of adsorbent on which the surfactant based on fluorinated acid or its salt is adsorbed with water; mixing particles of the adsorbent on which the surfactant based on fluorinated acid or its salt is adsorbed with alcohol or inorganic acid in the presence of water, initiation of etherification of the said surfactant based on fluorinated acid or its salt with the said alcohol to obtain an ether derivative of the said fluorinated surfactant, distillation of the said mixture to obtain a distillate containing the said ether derivative, separation of the said ether derivative from the said distillate and optional return of the remaining distillate to the said mixture and optional conversion of the said ether derivative to the corresponding surfactant based on fluorinated acid or its salt.

EFFECT: efficient method enables use of minimal amount of regenerating liquid and leads to obtaining regenerated particles of adsorbent which can be used repeatedly.

8 cl, 18 ex

Similar patents RU2382762C2

Title Year Author Number
REMOVAL OF FLUORINE-CONTAINING SURFACTANTS FROM WASTE WATER 2005
  • Khinttser Klaus
  • Obermaier Ehgon
  • Shvertfeger Verner
RU2397148C2
METHOD OF PURIFYING FLUORINATED COMPOUND 2009
  • Takagi Khirokazu
  • Seki Riudzi
RU2510713C2
METHOD OF REGENERATING BASIC ION EXCHANGE RESIN 2006
  • Khiguti Sinia
  • Khosikava Dzun
  • Kamija Khiroki
  • Matsuoka Jasukhiko
  • Funaki Khirosi
RU2388537C2
METHOD OF REGENERATION OF THE FLUORINE-CONTAINING EMULSIFIER 2003
  • Funaki Khirosi
  • Janase Koiti
  • Kamija Khiroki
  • Uekhara Masao
  • Nagatomo Kenitiro
  • Nisimura Jasusi
  • Okhno Siro
  • Khirano Satoru
RU2315718C2
METHOD FOR REMOVING PERFLUORINATED ALKANOIC ACIDS 2017
  • Zipplies, Tilman, C.
  • Hintzer, Klaus
  • Traunspurger, Helmut
  • Weilandt, Karl, D.
RU2686205C1
METHOD FOR RECOVERY OF FLUORINE-CONTAINING EMULSIFIER FROM AQUEOUS PHASE 2000
  • Burkard Georg
  • Khinttser Klaus
  • Ler Gernot
RU2248328C2
PROCESS DECREASING AMOUNT OF FLUORO-CONTAINING SURFACTANT IN AQUEOUS FLUOROPOLYMERIC DISPERSIONS 2003
  • Epsh Rebekka
  • Khintzer Klaus
  • Ler Gernot
  • Shvertfeger Verner
RU2319712C2
METHOD OF REGENERATING FLUORINATED ALKANE ACIDS FROM WASTE WATERS 1999
  • Feliks Bernd
  • Tsipplis Til'Man
  • Fjurer Shtefan
  • Kajzer Tomas
  • Budeskhajm Armin
RU2224721C2
METHOD OF PRODUCING FLUOROPOLYMERS 2009
  • Markionni Dzhuzeppe
  • Tortelli Vito
  • Vlassiks Ivan
  • Kapeljushko Valerij Ivanovich
RU2497836C2
METHOD OF RECOVERING FLUORINATED ALKANE ACIDS FROM WASTE WATERS 1999
  • Feliks Bernd
  • Zul'Tsbakh Rajnkhard
  • Fjurer Shtefan
  • Kajzer Tomas
  • Knip Khagen
  • Budeskhajm Armin
RU2226186C2

RU 2 382 762 C2

Authors

Fuerer Stefan

Khinttser Klaus

Ler Gernot

Obermajer Ehgon

Shvertfeger Verner

Dates

2010-02-27Published

2005-01-14Filed