FIELD: chemistry.
SUBSTANCE: method for quantitative chemiluminescent determination of ω-chloracetophenon in organic extracts involves treatment of the solution of a sample with potassium hydroxide solution, alkaline solution of luminol and hemin solution in a aqueous-alcoholic medium at temperature of 293 K and volume ratio of 1:1:1:1 respectively, with subsequent determination of chemiluminescence intensity of the sample compared to the control and determination of content of ω-chloracetophenon using a calibration curve.
EFFECT: increased sensitivity and faster analysis.
1 ex, 3 dwg, 1 tbl
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Authors
Dates
2010-04-10—Published
2007-10-12—Filed