FIELD: chemistry.
SUBSTANCE: invention relates to atomic industry and can be applied in technological processes of obtaining uranium tetrafluoride and in production of metallic uranium. Method of obtaining uranium tetrafluoride includes dissolution of uranium dioxide, sedimentation of uranium tetrafluoride from obtained solution by supplying hydrofluoric acid. After that carried out are pulp filtration, sediment washing, drying and burning. Dissolution of uranium dioxide is carried out in mixed solution of hydrochloric and hydrofluoric acids obtaining solution of complex uranium compound with uranium concentration up to 480 g/l. Uranium tetrafluoride from solution is precipitated in form of crystal hydrate by dosed supply of hydrofluoric acid during 15-30 min, without forced heating of reaction medium.
EFFECT: increase of process productivity and reduction of expenditures.
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Authors
Dates
2010-08-10—Published
2008-07-24—Filed