FIELD: chemistry.
SUBSTANCE: halogen used is bromine or iodine, and sulphuric anhydride is used in form of its solution in sulphuric acid with concentration of 5-60%. The chemical treatment process is carried out at temperature of 20-80°C, preferably at 50-70°C, with weight ratio of the sulphuric anhydride to halogen equal to 1-10:1, preferably 1.5-3:1.
EFFECT: obtaining highly pure product.
3 cl, 4 ex
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Authors
Dates
2010-11-27—Published
2009-03-18—Filed