METHOD OF PRODUCING PERFLUOROALKYNE COMPOUND Russian patent published in 2011 - IPC C07C17/23 C07C21/22 

Abstract RU 2422426 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing a perfluoroalkyne compound comprising a step for adding Cl2, Br2 or l2 to a compound of formula (1) CH3C≡CR1 to obtain a compound of formula (2) CH3CX2CX2R1, a step for fluorinating the compound of formula (2) with fluorine gas to obtain a compound of formula (3) CF3CX2CX2R2, and a dehalogenation step - reaction of the compound of formula (3) with a metal or organometallic compound to obtain a perfluoroalkyne compound of formula (4) CF3C≡CR2. In the formulae given above, R1 is a methyl or ethyl group, X is O, Br or I, and R2 is a trifluoromethyl group or a pentafluoroethyl group.

EFFECT: high efficiency and high output of the end product using starting materials which are ecologically clean and industrially accessible.

3 cl, 1 ex

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RU 2 422 426 C2

Authors

Sugimoto Tatsuja

Dates

2011-06-27Published

2007-03-30Filed