FIELD: oil and gas production.
SUBSTANCE: here is disclosed demulsifier of resin kind for breaking emulsion of water-in-oil type. Demulsifier contains oxy-ethylated product of inter-phase condensation of alkyl-phenol with number of carbon atoms in alkyl radical C8-C12 with formaldehyde corresponding to 4-6-nucleus novolak, organic dissolver and SAS (surface active substance) chosen from a row of aryl- or alkyl-sulphonates at the following ratio of components (wt, shares): oxy-ethylated product of condensation - 70.0-80.0; SAS - 0.05-0.5; organic dissolvent - up to 100. Also, here is disclosed the device for breakdown of oil-water emulsions corresponding to the above described demulsifier and procedure for production of demulsifier of resin kind for breaking emulsions of water-in-oil type. The procedure consists in inter-phase condensation of alkyl-phenol with number of carbon atoms in alkyl radical C8-C12, with formaldehyde at presence of surface-active substance (SAS) chosen from the row of aryl- or alkyl-sulphonates, acid catalyst with pKa>2 and organic dissolvent, in heating, in separation of water phase and in obtaining product of inter-phase condensation corresponding to 4-6 nucleus novolak. The latter is oxy-ethylated at presence of alkali catalyst.
EFFECT: raised degree of transformation and degree of alkyl-phenol condensation.
9 cl, 6 ex, 2 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING DEMULSIFIER FOR DESTRUCTING AQUEOUS CRUDE OIL EMULSIONS | 2000 |
|
RU2179994C1 |
METHOD OF PREPARING WATER-OIL EMULSION DEMULSIFIER PREVENTING FORMATION OF ASPHALT-TAR-PARAFFIN DEPOSITS AND OIL-FIELD EQUIPMENT CORROSION | 2005 |
|
RU2301254C2 |
COMPOSITION FOR DESTROYING STABLE WATER-OIL EMULSIONS AND PROTECTING OIL-FIELD EQUIPMENT AGAINST ASPHALTENE-TAR-PARAFFIN DEPOSITS | 2001 |
|
RU2184129C1 |
COMPOSITION FOR BREAKDOWN OF STABLE WATER-AND- OIL EMULSIONS AND PROTECTION OF OIL FIELD EQUIPMENT AGAINST ASPHALT-GUM-PARAFFIN DEPOSITS AND CORROSION | 2002 |
|
RU2227154C2 |
METHOD OF PREPARING DEMULSIFIER FOR WATER-OIL EMULSION RUPTURE | 1992 |
|
RU2043389C1 |
COMPOSITION FOR DESTRUCTION OF WATER-OIL EMULSIONS AND PROTECTION OF OIL FIELD EQUIPMENT FROM ASPHALTENE-RESIN-PARAFFIN DEPOSITS AND CORROSION | 2001 |
|
RU2185400C1 |
METHOD OF PRODUCING DEMULSIFIER FOR DECOMPOSITION OF WATER-OIL EMULSIONS | 1992 |
|
RU2037511C1 |
DEMULSIFIER PREPARATION METHOD | 2001 |
|
RU2186088C1 |
COMPOSITION FOR BREAKING DOWN WATER-OIL EMULSIONS AND PROTECTING OIL FIELD EQUIPMENT FROM CORROSION | 2013 |
|
RU2549534C1 |
COMPOSITION FOR DESTRUCTING AQUEOUS OIL EMULSION, PROTECTION OF OIL PRODUCTION EQUIPMENT FROM CORROSION AND PREVENTION OF ASPHALTENE-RESIN-PARAFFIN DEPOSITIONS (VARIANTS) | 1994 |
|
RU2096438C1 |
Authors
Dates
2011-06-27—Published
2010-03-23—Filed