FIELD: chemistry.
SUBSTANCE: invention can be used in production of silicon semiconductor. Trichlorosilane obtained via hydrochlorination of technical silicon is purified from high-boiling compounds, including methylchlorosilane, through distillation in one column with concentration ratio of trichlorosilane to methylchlorosilane in the residue equal to 23-30.
EFFECT: invention enables to obtain trichlorosilane with methylchlorosilane content of not more than 8,4·10-6 wt % and output of up to 98%.
1 tbl, 9 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR SEPARATION OF DIRECT TRICHLOROSILANE SYNTHESIS PRODUCTS | 2007 |
|
RU2358907C1 |
METHOD OF PRODUCTION 0F TRICHLOROSILANE | 2004 |
|
RU2280010C1 |
METHOD OF ISOLATING HIGH-PURITY TRICHLOROSILANE FROM REACTION MIXTURE OF METHYLCHLOROSILANES | 2007 |
|
RU2341457C1 |
METHOD OF PRODUCING TRICHLOROSILANE | 2008 |
|
RU2394762C2 |
METHOD OF PRODUCTION OF CHLOROSILANE | 2002 |
|
RU2214363C1 |
METHOD OF PRODUCTION OF TRICHLOROSILANE | 2003 |
|
RU2254291C1 |
POLYCRYSTALLINE SILICON PROCESS | 2007 |
|
RU2357923C2 |
METHOD OF SEPARATING TRICHLOROSILANE AND SILICON TETRACHLORIDE FROM MIXTURE OF CHLOROSILANES | 0 |
|
SU1597341A1 |
METHOD OF OBTAINING POLYCRYSTALLINE SILICON | 2018 |
|
RU2674955C1 |
METHOD OF PRODUCTION OF TRICHLOROSILANE | 2002 |
|
RU2214364C1 |
Authors
Dates
2011-08-20—Published
2010-02-02—Filed