METHOD OF PRODUCING D(+) GLUCOSAMINE HYDROCHLORIDE Russian patent published in 2012 - IPC C07H5/04 C08B37/08 A61K31/7008 

Abstract RU 2440362 C1

FIELD: chemistry.

SUBSTANCE: method involves preliminary acetylation of chitin with acetic anhydride, washing and drying the acetylated chitin in order to reduce degree of deacetylation thereof and, as a result, increase output of the desired product - D(+)-glucosamine hydrochloride when obtaining said product through hydrolysis of acetylated chitin with concentrated hydrochloric acid while heating, followed by evaporation, crystallisation, separation, washing and drying the desired product.

EFFECT: high output of the desired product while maintaining its high quality; method is more environmentally friendly since pre-treatment of chitin reduces the amount of processing wastes.

1 cl, 2 ex

Similar patents RU2440362C1

Title Year Author Number
METHOD OF SYNTHESIS OF D(+)-GLUCOSAMINE 1992
  • Novikov V.Ju.
  • Ivanov A.L.
RU2042685C1
METHOD OF PREPARING ANTIARTHROSIS MEDICINAL PREPARATION - GLUCOSAMINE HYDROCHLORIDE 1998
  • Novikov V.Ju.
  • Chilingarjan G.G.
  • Kompantsev V.A.
  • Samokish I.I.
RU2141964C1
METHOD FOR PRODUCING GLUCOSAMINE HYDROCHLORIDE POSSESSING ANTIARTHROSIS ACTIVITY 1991
  • Kazakov A.L.
  • Samokish I.I.
  • Kompantsev V.A.
  • Lobova E.I.
  • Novikov V.Ju.
  • Orlova T.A.
RU2038095C1
COMPOSITIONS OF PARTIALLY DEACETYLATED CHITIN DERIVATIVES 2006
  • Dzhislejzon Jokhannes
  • Ajnarsson Jon M.
  • Chuen Khau Ng
  • Barke Sven
RU2421467C2
METHOD FOR WASTELESS COMPLEX REPROCESSING OF CHITIN-CONTAINING RAW MATERIAL 2000
  • Novikov V.Ju.
  • Mukhin V.A.
  • Chilingarjan G.G.
RU2207033C2
METHOD OF CHITOSAN PRODUCTION FROM CRUSTACEA CRUSTS 2006
  • Novikov Vitalij Jur'Evich
  • Chebotok Elena Nikolaevna
RU2332081C1
METHOD OF PREPARING GLUCANE-CHITOSAN COMPLEX 1992
  • Teslenko A.Ja.
  • Voevodina I.N.
  • Galkin A.V.
  • L'Vova E.B.
  • Nikiforova T.A.
  • Nikolaeva S.V.
  • Mikhajlov B.V.
  • Kozlov V.P.
RU2043995C1
METHOD OF OBTAINING CHITOSAN 2009
  • Bristov Dzhozef
RU2548178C2
METHOD FOR DEACETYLATION OF BIOPOLYMERS 2016
  • Olsson, Yukhan
  • Kharris, Krejg Stiven
RU2748235C2
CHITOSAN CARBOXYALKYLAMIDE HYDROGEL, PREPARING IT AND USING IN COSMETOLOGY AND DERMATOLOGY 2008
  • Lozh'E Ehlizabet
  • Gushe Frank
  • Perro Zhan-P'Er
RU2476201C2

RU 2 440 362 C1

Authors

Novikov Vitalij Jur'Evich

Dolgopjatova Natal'Ja Vladimirovna

Dates

2012-01-20Published

2010-05-25Filed