FIELD: process engineering.
SUBSTANCE: invention relates to activation of metal oxide catalysts. Proposed method uses oxides of VIII-group metals as catalysts and consists in that salts of VIII-group metals and magnesium nitrate are used as initial material and decomposed by thermal decomposition of precursor water solution. Prior to calcination, the latter is subjected to effects of super high frequency fields with circular polarisation at 2.45 GHz fir 5-40 s. Thereafter, said solution is calcinated at 600-650°C for 30 min.
EFFECT: higher yield of nanotubes.
4 dwg
Title | Year | Author | Number |
---|---|---|---|
METHOD OF ACTIVATING METAL OXIDE CATALYSTS FOR SYNTHESIS OF CARBON NANOMATERIALS | 2009 |
|
RU2430779C2 |
METAL OXIDE CATALYSTS FOR GROWING CARBON NANOTUBES FROM GAS PHASE | 2009 |
|
RU2415706C1 |
METHOD OF OBTAINING METAL OXIDE CATALYSTS FOR GROWING CARBON NANOTUBES FROM GASEOUS PHASE | 2010 |
|
RU2476268C2 |
METHOD OF PRODUCING FINE-GRAINED SUPPORTED CATALYSTS AND SYNTHESIS OF CARBON NANOTUBES | 2008 |
|
RU2373995C1 |
COBALT-BASED CATALYSTS ACTIVATION PROCESS | 2002 |
|
RU2301110C2 |
METAL-OXIDE CATALYST FOR GROWING BUNDLES OF CARBON NANOTUBES FROM GASEOUS PHASE | 2010 |
|
RU2427423C1 |
METHOD OF REGENERATING FISCHER-TROPSCH SYNTHESIS COBALT CATALYST | 2008 |
|
RU2456080C2 |
PROCEDURE FOR FABRICATING LONG ORIENTED BRAIDS OF CARBON NANO-FIBRES | 2009 |
|
RU2393276C1 |
METHOD OF PRODUCING SUPPORTED COBALT-BASED FISCHER-TROPSCH SYNTHESIS CATALYST | 2008 |
|
RU2458100C2 |
METHOD OF PREPARING SUPPORTED COBALT-BASED FISCHER-TROPSCH SYNTHESIS CATALYST | 2008 |
|
RU2456329C2 |
Authors
Dates
2012-02-27—Published
2010-03-09—Filed