METHOD OF PRODUCING (ACETYLACETONATO-κ-O,O')(BIS-ACETONITRILE)PALLADIUM TETRAFLUOROBORATE Russian patent published in 2012 - IPC C07F15/00 C07F5/02 

Abstract RU 2456295 C1

FIELD: chemistry.

SUBSTANCE: present invention relates to a method of producing (acetylacetonato-k2-O,O')(bis-acetonitrile)palladium tetrafluoroborate (where acac denotes acetyl acetonate, MeCN denotes acetonitrile). The method involves reaction of bis(acetylacetonato)palladium Pd(acac)2 with acetonitrile and a boron compound in the medium of an organic solvent at room temperature. The boron compound used is boron trifluoride etherate BF3·OEt2, the organic solvent used is aromatic solvents, specifically benzene or toluene.

EFFECT: invention increases output of (acetylacetonato-k2-O,O')(bis-acetonitrile)palladium tetrafluoroborate.

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RU 2 456 295 C1

Authors

Suslov Dmitrij Sergeevich

Tkach Vitalij Sergeevich

Bykov Mikhail Valer'Evich

Belova Marina Vladimirovna

Dates

2012-07-20Published

2011-03-31Filed