FIELD: chemistry.
SUBSTANCE: invention relates to an improved method of producing fatty acid esters, which are used as diesel biofuel, from whole oilseeds, involving the following consecutive steps: a) preheating unhulled and cleaned whole seeds; b) squashing the oilseeds together with their shells; c) drying the squashed seeds until achieving water and volatile substance content of 0.5-2.5%; d) re-esterification by bringing the squashed seeds into contact with an alcohol medium in the presence of a catalyst; e) separating the liquid and solid phases obtained from re-esterification; f) neutralising the liquid phase obtained at step (e); and g) removing alcohol and separating glycerol from fatty acid esters, which are then purified. The invention also relates to a method of producing an oil cake, meant for use as animal feed, from the obtained solid phase, which involves the following steps: 1) removing alcohol from said solid phase; and 2) adding glycerol obtained at step (g) of the method on any of the previous claims.
EFFECT: method of obtaining fatty acid esters from squashed oilseeds.
25 cl, 12 tbl, 19 ex
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Authors
Dates
2013-04-10—Published
2008-07-24—Filed