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2 484 010

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(51)

IPC

C01B31/00(2006-01-01)

C07B61/00(2006-01-01)

C07C23/00(2006-01-01)

C07C247/14(2006-01-01)

(21) (22)

Application

2011124692/05, 2011-06-16

(24)

Start date

2011-06-16

(22)

Actual filing date

2011-06-16

(45)

Published

2013-06-10

(72)

Inventor

Dzhemilev Usein MemetovichTuktarov Ajrat RamilevichAkhmetov Arslan RifkhatovichJarullin Il'Dar RafisovichGabidullina Linara Akhmedovna

(73)

Holder

Uchrezhdenie Rossijskoj Akademii Nauk Institut Neftekhimii I Kataliza Ran

METHOD OF PRODUCING 1-IODO-2-AZIDO(C-I)[5,6]FULLERENE Russian patent published in 2013 - IPC C01B31/00 C07B61/00 C07C23/00 C07C247/14

Abstract RU 2484010 C2

FIELD: chemistry.

SUBSTANCE: invention relates to organic synthesis and specifically to a method of producing functionally substituted fullerenes which can be used as donor-acceptor systems. The method of producing 1-iodo-2-azido(C₆₀-I_h)[5,6]fullerene involves reaction of fullerene C₆₀ with iodine azide, taken in molar ratio C₆₀:IN₃=1:(10-30), at room temperature (20°C) in chlorobenzene for 2-4 hours under a current of dry argon without access to daylight.

EFFECT: invention provides selective production of 1-iodo-2-azido(C₆₀-I_h)[5,6]fullerene.

1 tbl

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RU 2 484 010 C2

Authors

Dzhemilev Usein Memetovich

Tuktarov Ajrat Ramilevich

Akhmetov Arslan Rifkhatovich

Jarullin Il'Dar Rafisovich

Gabidullina Linara Akhmedovna

Dates

2013-06-10—Published

2011-06-16—Filed