FIELD: chemistry.
SUBSTANCE: invention can be used in electronics, material science, instrument-making, metrology, information technology, chemistry, ecology, biology and medicine. Initial product of electric arc synthesis is separated into light and heavy fractions by distillation in "boiling layer" mode or by floatation. For "boiling layer" mode air is used as carrier-gas and is supplied at rate, which provides mode of laminar flow of light fraction. Sodium nitrate solution with specific weight 1.26-1.37 g/cm3 is used as floatation liquid. Heavy fraction is processed with concentrated hydrochloric acid and ultrasound, washed, dried and successively oxidised with air oxygen at 450 °C and 600 °C with intermediate processing with concentrated hydrochloric acid and ultrasound, washing and drying until constant weight is obtained.
EFFECT: reduction of process duration, improved quality of separated nanotubes due to reduction in them of metal and amorphous carbon.
4 dwg, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PURIFICATION OF SINGLE-WALLED CARBON NANOTUBES | 2022 |
|
RU2799992C1 |
METHOD OF PRODUCING IODINE-DOPED CARBON NANOTUBES | 2018 |
|
RU2687447C1 |
METHOD OF PRODUCING HIGH-STRENGTH COMPOSITE MATERIAL BASED ON A THERMOPLASTIC POLYMER, A MODIFIER FOR PREPARING A COMPOSITE MATERIAL AND A METHOD OF PRODUCING A MODIFIER FOR PREPARING COMPOSITE MATERIAL (VERSIONS) | 2019 |
|
RU2708583C1 |
MODIFYING ADDITIVE TO ASPHALT CONCRETE | 2023 |
|
RU2801276C1 |
LITHIUM-ION BATTERY CATHODE MANUFACTURING METHOD | 2024 |
|
RU2824454C1 |
METHOD FOR PREPARING ANODE PASTE FOR LITHIUM-ION BATTERY, ANODE PASTE, METHOD FOR MANUFACTURE OF ANODE (VARIANTS), ANODE (VARIANTS) AND LITHIUM-ION BATTERY (VARIANTS) | 2020 |
|
RU2749904C1 |
POLYMER AND CARBON NANOTUBES BASED HYBRID ELECTRIC CONDUCTING MATERIAL AND ITS PRODUCTION METHOD | 2017 |
|
RU2665394C1 |
HYBRID MATERIAL BASED ON POLY-3-AMINO-7-METHYLAMINE-2-METHYLPHENAZINE AND SINGLE-WALLED CARBON NANOTUBES AND METHOD OF ITS PRODUCTION | 2016 |
|
RU2635606C2 |
CARBON NANOTUBE DISPERSION, DISPERSION PREPARATION METHOD, CATHODE PASTE, CATHODE PRODUCTION METHOD AND CATHODE | 2021 |
|
RU2777379C1 |
HYBRID MAGNETIC AND ELECTROCONDUCTIVE MATERIAL BASED ON POLYMER, BIMETALLIC NANOPARTICLES AND CARBON NANOTUBES, AND METHOD FOR PRODUCTION THEREOF | 2019 |
|
RU2737184C1 |
Authors
Dates
2013-08-20—Published
2011-08-30—Filed