FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing palladium (II) beta-ketoiminates. The method involves reacting palladium dichloride with a beta-ketoiminate. The palladium dichloride in aqueous solution of concentrated ammonia (NH3(concentrated):H2O - 25:25 ml) is transferred into an ampoule which is then placed in a microwave oven reactor and excess beta-ketoimine (in ratio of 1:(2-3)) dissolved in ethanol is then added. The mixture is exposed to 100-150 W microwaves to heat the solution for 2-30 minutes at temperature of 90-110°C. The end product is separated by filtration and the residue is dried on air.
EFFECT: simple method, shorter duration of the method, high output of end products.
2 cl, 3 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING PALLADIUM (II) BETA-DIKETONATE OR BETA-KETOIMINATE | 2012 |
|
RU2513021C1 |
| METHOD FOR PRODUCTION OF TRIS(2,7-OCTADIENYL)AMINE | 2006 |
|
RU2318798C1 |
| METHOD OF PRODUCING BETA-DIKETONATE OF PALLADIUM (II) | 2016 |
|
RU2641893C1 |
| METHOD OF OBTAINING CATIONIC PALLADIUM COMPLEXES | 2011 |
|
RU2466134C1 |
| COMPOUNDS ON THE BASIS OF PALLADIUM AND AROMATIC AMINE DERIVATIVES, AND A METHOD OF THEIR SYNTHESIS | 1992 |
|
RU2022968C1 |
| METHOD OF PRODUCING METAL-APPLIED CATALYST FOR PROCESS OF PHOTOCATALYTIC OXIDATION OF CARBON MONOXIDE | 2016 |
|
RU2637120C1 |
| FUROPYRIDINES AS BROMODOMAIN INHIBITORS | 2014 |
|
RU2655727C9 |
| METHOD OF PRODUCING 4-METHOXYBIPHENYL BY A SUZUKI REACTION USING BIMETALLIC PD-CONTAINING CATALYSTS | 2020 |
|
RU2736719C1 |
| METHOD TO PRODUCE PALLADIUM SOLUBLE IN NITRIC ACID | 2010 |
|
RU2463366C2 |
| METHOD FOR OBTAINING PALLADIUM ANILINE COMPLEXES | 2015 |
|
RU2618526C1 |
