METHOD OF OBTAINING META-CHLOROBENZOPHENONE AS HALF-PRODUCT OF ANTICONVULSIVE MEDICATION "HALODIF" Russian patent published in 2014 - IPC C07C49/813 C07C45/65 

Abstract RU 2510638 C1

FIELD: chemistry.

SUBSTANCE: meta-chlorobenzophenone is obtained by diazotization of 2-amino-5-chlorobenzophenone at room temperature. Diazotization is carried out in mixture of icy acetic and hydrochloric acids with application of water solution of sodium nitrate with the following processing of obtained salt of diazonium with water solution of sodium hypophosphite or copper protoxide in ethyl alcohol for 0.5-1 h.

EFFECT: method makes it possible to realise process at room temperature, reduce its duration and obtain meta-chlorobenzophenone with high output.

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RU 2 510 638 C1

Authors

Shtrykova Viktorija Viktorovna

Filimonov Viktor Dmitrievich

Kuksenok Vera Jur'Evna

Dates

2014-04-10Published

2012-12-03Filed