METHOD FOR OBTAINING METALLIC RHENIUM BY REDUCTION OF AMMONIUM PERRHENATE Russian patent published in 2014 - IPC C22B61/00 

Abstract RU 2511549 C1

FIELD: metallurgy.

SUBSTANCE: method for obtaining metallic rhenium by reduction of ammonium perrhenate involves arrangement of ammonium perrhenate powder in a boat and its reduction by counter current of dry hydrogen with continuous movement of the boat in a tube furnace at the temperature of 300-330°C. Prior to reduction, ammonium perrhenate powder is purged with argon and heated in the tube furnace up to the temperature of 200°C.

EFFECT: method ensures production of rhenium powder that requires no cleaning from impurities, as well as reduction of rhenium powder losses.

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Authors

Anikin Vjacheslav Nikolaevich

Konokov Gennadij Khadzhimusovich

Zolotareva Natal'Ja Nikolaevna

Anikeev Aleksandr Ivanovich

Belokopytova Kristina Evgen'Evna

Tambovtseva Alla Aganesovna

Luk'Janychev Sergej Jur'Evich

Anikin Grigorij Vjacheslavovich

Anikina Tat'Jana Georgievna

Krjuchkov Konstantin Viktorovich

Dates

2014-04-10Published

2013-02-07Filed