FIELD: metallurgy.
SUBSTANCE: method for obtaining metallic rhenium by reduction of ammonium perrhenate involves arrangement of ammonium perrhenate powder in a boat and its reduction by counter current of dry hydrogen with continuous movement of the boat in a tube furnace at the temperature of 300-330°C. Prior to reduction, ammonium perrhenate powder is purged with argon and heated in the tube furnace up to the temperature of 200°C.
EFFECT: method ensures production of rhenium powder that requires no cleaning from impurities, as well as reduction of rhenium powder losses.
1 tbl, 1 ex
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Authors
Dates
2014-04-10—Published
2013-02-07—Filed