FIELD: chemistry.
SUBSTANCE: invention relates to field of organic chemistry, namely to method of obtaining N-(1,5,3-dithiazonan-3-yl)amides of general formula (1): 
where R=p-C5H4N (a), (CH3)3CO (b), m-C5H4N (c), which consists in the following: hydrazides of general formula RC(O)NHNH2 (R=mentioned above) undergo interaction with 1,4-butanedithiol, preliminarily mixed at 20°C with water formaldehyde solution, in presence of catalyst crystallohydrate of copper chloride CuCl2·2H2O with molar ration 1,4-butanedithiol: CH2O : RC(O)NHNH2 : CuCl2·2H2O = 10:20:10:(0.3-0.7) at 75-85°C and atmospheric pressure for 44-52 h.
EFFECT: elaborated is method of obtaining novel compounds, which can be applied as biologically active compounds, selective sorbents and extractants of noble and precious metals.
1 tbl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF OBTAINING N-(1,5,3-DITHIAZONAN-3-YL)AMIDES | 2012 |
|
RU2516696C1 |
| METHOD OF PRODUCING N-(1,5,3-DITHIAZOCYNAN-3-YL)AMIDES | 2011 |
|
RU2565788C2 |
| METHOD OF PRODUCING N-(1,5,3-DITHIAZEPAN-3-YL)AMIDES | 2011 |
|
RU2478626C1 |
| METHOD OF PRODUCING N-(1,5,3-DITHIAZEPINAN-3-YL)AMIDES | 2011 |
|
RU2481338C1 |
| METHOD FOR PREPARING N-(1,5,3-DITHIAZOCYNAN-3-YL)AMIDES | 2012 |
|
RU2496777C2 |
| METHOD OF PRODUCING N-(1,5,3-DITHIAZEPAN-3-YL)AMIDES | 2011 |
|
RU2482114C2 |
| METHOD OF PRODUCING N-ARYL-1,5,3-DITHIAZONANES | 2014 |
|
RU2559361C1 |
| METHOD OF PRODUCING N',N'-BIS{[N-ALLYL(THIO)CARBAMOYL METHYL]}ARYL HYDRAZIDES | 2013 |
|
RU2551686C1 |
| METHOD OF PRODUCING N',N'-BIS{[ALKYL(PHENYL)SULPHANYL]METHYL}ARYLHYDRAZIDES | 2012 |
|
RU2504537C2 |
| METHOD OF OBTAINING N', N'-BIS{[ALKYL(PHENYL)SULFANYL]METHYL} ARYL HYDRAZIDES | 2012 |
|
RU2518491C2 |
