FIELD: chemistry.
SUBSTANCE: present invention relates to a method of producing polyalkylene glycol di(meth)acrylates. Described is a method of producing polyalkylene glycol di(meth)acrylates by reacting polyalkylene glycol with (meth)acrylic anhydride, wherein the polyalkylene glycol has weight-average molecular weight ranging from 1000 to 10000 g/mol, the reaction mixture is free of metal compounds and/or amines and solvents, the reaction is carried out in the presence of polymerisation inhibitors and the reaction temperature ranges from 70°C to 120°C and the obtained reaction mixture is treated by adding water, wherein the ratio of the weight of the treated reaction mixture to water ranges from 5:1 to 1:5.
EFFECT: obtaining polyalkylene glycol di(meth)acrylates, characterised by cost-effectiveness, high selectivity and absence of catalyst residues in the product.
12 cl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
USING SWELLABLE POLYMER FOR SEALING | 2008 |
|
RU2496795C2 |
MACROMONOMERS CONTAINING POLYISOBUTENE GROUPS AND THEIR HOMO- AND COPOLYMERS | 2017 |
|
RU2745788C2 |
METHOD OF OBTAINING (MET)ACRYLIC ACID ETHERS | 2009 |
|
RU2515985C2 |
METHOD FOR OBTAINING THE MODIFIED EPOXIES OF (METH) ACRYLATE RESINS AND THEIR APPLICATION | 2013 |
|
RU2648042C2 |
METHOD OF PRODUCING ALKOXY-POLYOXYALKYLENE(METH)ACRYLATES | 2007 |
|
RU2440970C2 |
METHOD OF PRODUCING A (MET)ACRYLIC ACID ESTER AND THE METHOD OF PRODUCTION OF AN AROMATIC CARBOXYLIC ACID ESTER | 2015 |
|
RU2661899C2 |
METHOD OF PRODUCING CARBOXYLIC ACID DERIVATIVES | 2007 |
|
RU2448949C2 |
METHOD OF OBTAINING CARBOXYLIC ACID AMIDE FROM CARBONYL COMPOUND AND HYDROCYANIC ACID | 2009 |
|
RU2552619C9 |
COSMETIC COMPOSITION INCLUDING, AT LEAST, ONE COPOLYMER OF SILICONE AND ACRYLATE AND, AT LEAST, ONE GRAFTED SILICONE COPOLYMER | 2000 |
|
RU2197221C2 |
METHOD OF CONTINUOUS PRODUCTION OF ALKYLAMINO(METH)ACRYLAMIDES | 2004 |
|
RU2374221C2 |
Authors
Dates
2014-07-10—Published
2009-05-05—Filed