FIELD: chemistry.
SUBSTANCE: invention relates to a method of treating an active Fischer-Tropsch catalyst and an apparatus for preparing and treating said catalyst. The method of treating an active catalyst includes loading a mixture of particles of an active Fischer-Tropsch catalyst and molten wax, which is at a temperature T1 and which sets at a lower temperature T2 lying between 70°C and 140°C, where T2<T1, into a plurality of moulds; at least partial immersion of the moulds into a cooling liquid to cool the organic substance to a temperature T3, where T3≤T2, to obtain cast products in form of candles with a volume of less than 140 ml but more than 2 ml each, having an organic substance matrix in which particles of the active catalyst are dispersed such that the catalyst particles are coated with wax; removing the cast products from the moulds; loading the mixture into moulds, immersing the moulds into a cooling liquid and removing the cast products form the mould in a casting machine. The apparatus includes equipment for preparing or regenerating the catalyst, including a reservoir for applying a coating onto the catalyst; a transportation means for transferring the mixture of particles of the active catalyst and molten organic substance from the reservoir for applying a coating onto the catalyst; a casting machine for producing cast products in form of candles which includes a plurality of moulds into which the transportation means can unload the mixture of particles of the active catalyst and molten organic substance, and a cooling bath capable of holding a cooling liquid into which the moulds can be immersed at least partially.
EFFECT: method and apparatus enables to safely and easily move a catalyst from the production site to the point of use without losing activity.
18 cl, 3 dwg, 3 tbl, 3 ex
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Authors
Dates
2014-09-20—Published
2010-05-20—Filed