FIELD: chemistry.
SUBSTANCE: invention relates to producing chitosan from chitin and can be used in medicine, chemical, textile, paper and food industry. The method comprises crushing chitin to particle size of 1-2×2-3 mm; deacetylation of chitin in a double-neck reactor in 40% NaOH solution with in ratio to chitin of (1-3):(20-60) at 100°C, pressure of 300 mm Hg for 1-2 hours, wherein the double-neck reactor is fitted with a reflux condenser and is connected to a vacuum water-jet pump.
EFFECT: invention improves the degree of acetylation of chitosan and preserves the natural structure of the finished product.
2 tbl, 1 dwg
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CHITIN PRODUCTION METHOD | 2012 |
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RU2382051C1 |
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RU2678125C1 |
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RU2067588C1 |
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RU2139887C1 |
Authors
Dates
2015-01-27—Published
2012-03-30—Filed