METHOD OF OBTAINING MONOMER FOR PROTON-CONDUCTING POLYMER MEMBRANES Russian patent published in 2015 - IPC C07C309/46 

Abstract RU 2547462 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of obtaining 2,2'-methylenebis[5-amino-4-methylbenzosulphoacid], which includes the sulphonation of 3,3'-dimethyl-4,4'-diaminodiphenylmethane with oleum at heating, the following extraction and purification of the target product by standard methods, which consists in the fact, that 3,3'-dimethyl-4,4'-diaminodiphenylmethane is applied in the form of a sulphate, obtained by the condensation of hydrochloride of o-toluidine with formaldehyde in a 10% solution of sulphuric acid, sulphate of 3,3'-dimethyl-4,4'-diaminodiphenylmethane after drying is subjected to interaction with 65% oleum at the weight ratio of reagents of 1:1.5 respectively.

EFFECT: obtaining the said compound from available initial substances.

2 cl, 3 ex

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RU 2 547 462 C1

Authors

Ponomarev Igor' Igorevich

Razorenov Dmitrij Jur'Evich

Ponomarev Ivan Igorevich

Volkova Julija Aleksandrovna

Zharinova Marina Jur'Evna

Skupov Kirill Mikhajlovich

Dates

2015-04-10Published

2014-03-13Filed