METHOD OF MANUFACTURING POWDER, CONTAINING ONE OR SEVERAL COMPLEXING SALTS Russian patent published in 2015 - IPC B01J2/04 C07C227/42 C11D3/33 C11D11/02 

Abstract RU 2554932 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method of obtaining powder, containing one or several complexing salts of the general formula in which R' stands for hydrogen or one of groupings or , with R" standing for hydrogen, alkyl residue with 1-12 carbon atoms or -(CH2)q-COOM residue, where q=1-5, n and m in each case represent an integer number from 0 to 5, and R"' represents hydrogen, or an alkyl residue with 1-12 carbon atoms, or an alkylene residue with 1-12 carbon atoms, which can be additionally substituted with hydroxyl groups in up to 5 in number, or one of groupings or , where o and p in each case represent an integer number from 0 to 5, and M independently on each other stands for an alkali metal, alkali earth metal, ammonium or substituted ammonium in respective stoichiometric amounts, and having the residual humidity in the range from 7 to 14 wt % relative to the total powder weight. The method is carried out basing on a water solution, which contains one or several complexing salts in a concentration from 10 to 80 wt % relative to the total weight of the water solution, by a method of spray drying, which includes a spray stage and a drying stage. The spray stage is carried out with the addition of crystalline finely-disperse dust of the same salt or the same complexing salts as those, contained in the water solution, or one or several different from them complexing salts, with the upper limit of the average particle diameter of the crystalline finely-disperse dust being at least two times smaller than the lower limit of the average diameter of the particle of the powder, obtained in accordance with the method, in an amount from 0.1 to 20 wt % relative to the weight of the powder, obtained in accordance with the method. The composition of washing and cleaning substances, application of the powder and pressed agglomerates are also claimed.

EFFECT: invention makes it possible to obtain the powder, possessing favourable indices of suitability for warehouse storage and to processing, which has higher degree of crystallinity and higher residual humidity un the range from 7 to 14 wt % relative to the total weight and possesses granulated shape.

13 cl, 4 dwg, 4 ex, 2 tbl

Similar patents RU2554932C2

Title Year Author Number
PRODUCTION OF PELLETS CONTAINING ONE OR SEVERAL COMPLEXING AGENT SALTS 2011
  • Blaj Shtefan
  • Shenkherr Mikhaehl'
  • Veber Frants
  • Bekker Fransua
RU2573412C2
METHOD FOR PRODUCING CRYSTALLINE SOLID FROM GLYCINE-N,N-DIACETIC ACID DERIVATIVES 2010
  • Baraniaj Andreas
RU2551851C2
SOLID SUBSTANCE CONTAINING GLUTAMIC ACID-N,N-DIACETIC ACID (GLDA) OR DERIVATIVE THEREOF, AS WELL AS METHOD FOR PRODUCTION THEREOF 2010
  • Baran'Jai Andreas
RU2560730C2
METHOD OF OBTAINING LOOSE POWDER, CONTAINING ONE OR SEVERAL GLYCIN-N,N-DIACETIC ACID DERIVATIVES, AND APPLICATION OF LOOSE POWDER FOR OBTAINING PRESSED AGGLOMERATES 2010
  • Mrtsena Frank
  • Shenkherr Mikhaehl'
  • Khajnts Robert
  • Khajdenfel'Der Tomas
RU2533974C2
POWDER AND GRANULE, PROCESS FOR MAKING SUCH POWDER AND GRANULE, AND USE THEREOF 2015
  • Khartmann Markus
  • Rajnozo Gartsia Marta
  • Myuller Mikhael Klemens
  • Ben Roland
  • Bil Markus Kristian
RU2678773C2
POWDERS AND GRANULES AND METHOD OF PRODUCING SUCH POWDERS AND GRANULES 2017
  • Myuller Mikhael Klemens
  • Shtamm Armin
  • Jekel Frank
  • Zyuling Karsten
RU2742268C2
METHOD OF PRODUCING GRANULES 2016
  • Jekel Frank
  • Myuller Mikhael Klemens
RU2728876C2
METHOD FOR PRODUCING GRANULES CONTAINING MGDA AND GLDA, GRANULES AND THEIR APPLICATION 2017
  • Rajnozo Garsia, Marta
  • Myuller, Mikhael Klemens
  • Zyuling, Karsten
  • Mormul, Ferena
RU2744632C2
MODIFIED AMINOCARBOXYLATES WITH IMPROVED STORAGE STABILITY AND PROCESSABILITY 2012
  • Lang Frank-Peter
  • Khartmann Markus
  • Garsiya Markos, Alekhandra
  • Khyuffer Shtefan
RU2608221C2
METHOD FOR PRODUCTION OF COMPLEX-FORMING AGENT 2018
  • Schmidt, Thomas
  • Stamm, Armin
  • Reinoso Garcia, Marta
  • Mormul, Verena
  • Mueller, Michael Klemens
  • Jaekel, Frank
  • Manning, Jeremy
RU2782828C2

RU 2 554 932 C2

Authors

Mrtsena Frank

Menge Ul'Rikh

Shenkherr Mikhaehl'

Khajdenfel'Der Tomas

Dates

2015-07-10Published

2010-10-11Filed