FIELD: chemistry.
SUBSTANCE: present invention relates to a method of regenerating a lanthanide catalyst from synthesis of diethoxysuccinate of aspartic acid. The method includes contacting a carbonate source with a solution containing lanthanide ions, formed during said synthesis, and a chelating agent, different from diethoxysuccinate of aspartic acid, for precipitation of a lanthanide carbonate followed by separation of the precipitated lanthanide carbonate from the solution, wherein said chelating agent is iminodisuccinic acid or ethylenediamine disuccinic acid. The invention also relates to a method of producing diethoxysuccinate of aspartic acid, which includes reacting diethanolamine with a maleate in alkaline conditions in the presence of a lanthanide catalyst.
EFFECT: improved regeneration of a lanthanide catalyst for synthesis of diethoxysuccinate of aspartic acid.
12 cl, 4 dwg, 4 tbl, 4 ex
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Authors
Dates
2015-07-10—Published
2011-05-31—Filed