FIELD: chemistry.
SUBSTANCE: invention relates to methods of producing organosilicon liquids. Disclosed is a method of producing oligodimethyl-γ-trifluoropropylsiloxane fluid as result of catalytic regrouping of initial combination consisting of (wt%): hexamethyldisiloxane (15±3), depolymerisate (32±5) and 1,3,5-trimethyl-1,3,5-tris(3,3,3-trifluoropropyl) cyclotrisiloxane (balance), in presence of sulfocationite (polistyrenedivinylbenzol sulphonated copolymer) in amount of 5±2 % to whole mass of starting composition, with further distillation of low-boiling fractions from product of catalytic rearrangement.
EFFECT: technical result is faster chemical process of fluid production and low level of losses of end product compared to existing methods.
3 cl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR OBTAINING MODIFIED POLYETHYLSILOXANE FLUIDS WITH IMPROVED LUBRICATING PROPERTIES | 2022 |
|
RU2787827C1 |
METHOD OF PRODUCING ORGANOFLUOROSILOXANE COPOLYMERS | 2011 |
|
RU2455319C1 |
0 |
|
SU477175A1 | |
CYCLOTRISILOXANE SYNTHESIS METHOD | 2008 |
|
RU2402577C2 |
METHOD OF PRODUCING LOW-MOLECULAR FLUORO-ORGANOSILOXANE POLYMERS | 2010 |
|
RU2440383C1 |
METHOD OF PREPARING OLIGOMETHYL-GAMMA-TRIFLUOROPROPYLSILOXANES | 2004 |
|
RU2268902C1 |
POLYMETHYL(HEXAFLUOROALKYL)SILOXANES FOR THERMO- AND OIL-BENZO-STABLE MATERIALS | 1995 |
|
RU2078097C1 |
METHOD OF PRODUCING α,ω - DIHYDROXYPOLYDIORGANOSILOXANES | 2019 |
|
RU2737804C1 |
METHOD OF OBTAINING POLYORGANOSILOXANES | 2007 |
|
RU2346960C1 |
0 |
|
SU469704A1 |
Authors
Dates
2016-05-20—Published
2015-02-20—Filed